Derivatization reagents for GC, silylation, MSHFBA, 5 × 10 mL

MSHFBA is used either alone or in combination with a catalyst (TMCS, TSIM) or another silylation reagent with or without solvent. The by-product N-methylheptafluorobutyric amide has a lower retention time than the silylating reagent. Especially useful for flame ionisation detection due to the large ratio of fluorine to silicon of 7:1, since degradation of the excess of MSHFBA does not produce SiO₂ but volatile, non-corrosive silicon compounds.

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Selling unit 5×10 mL
Method Gas chromatography (GC), derivatization
Composition N-methyl-N-trimethylsilyl-heptafluorobutyramide (MSHFBA)
Derivatization type Silylation
Recommended application(s) Alcohols, Amino acids, Carboxylic acids, Derivatization, Phenols, Primary and secondary amines
Storage temperature 2–8 °C / 36–46 °F
Hazardous material Yes
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